HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl 3-(2-(methylamino)ethyl)benzoate → Methyl 3-(2-((4-(3,4-dimethoxyphenyl)-4-(methoxycarbonyl)-5-methylhexyl)(methyl)amino)ethyl)benzoate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl 3-(2-(methylamino)ethyl)benzoate | HCID 59419935 | — |
| Reactant | Methyl 5-chloro-2-(3,4-dimethoxyphenyl)-2-isopropylpentanoate | HCID 59419939 | — |
| Product | Methyl 3-(2-((4-(3,4-dimethoxyphenyl)-4-(methoxycarbonyl)-5-methylhexyl)(methyl)amino)ethyl)benzoate | HCID 25130667 | — |
Reaction Steps
Reaction of 1e with 2d produced 3aj. MS found M+H=486. The oxalate salt of 3aj was recrystallized from ethyl acetate; mp 87-90° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09227918B2 |
| Source dataset | uspto-grants-2016_01 |
| ORD ID | ord-8cb2a99026e34ba3bb15f138fd13345a |
| Source note | uspto-grants-2016_01 |