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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 587981Generated: October 31, 2026

Triethyl phosphite → HCID 12565589, compound

https://huagongshe.com/reaction/587981

Reaction equation

Participants

RoleNameHCIDCharge
ReactantTriethyl phosphiteHCID 31215—
ReactantButanoic acid, 2-bromo-, methyl esterHCID 95577—
ProductHCID 12565589HCID 12565589—

Reaction Conditions

Temperature110 °C

Reaction Steps

Methyl 2-bromobutanoate (92 g, 0.508 mol) and triethylphosphite (95 g, 0.57 mol) were mixed, and the mixture was stirred at 110° C. for 3 days. The reaction mixture was dried under reduced pressure to give the title compound.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS09227949B2
Source datasetuspto-grants-2016_01
ORD IDord-e4d9383d4afb4a1aa648a281f2c23751
Source noteuspto-grants-2016_01