Morpholine → HCID 178513121, compound

HRID 589208Notes

Reaction equation

HRID 589208 reaction equation
I.[NH:2]([C:4](SC)=[NH:5])[NH2:3].[NH:8]1[CH2:13][CH2:12][O:11][CH2:10][CH2:9]1>CO>[N:8]1([C:4](=[NH:5])[NH:2][NH2:3])[CH2:13][CH2:12][O:11][CH2:10][CH2:9]1

Participants

4

Reactant 2

HCID 8083MorpholineHCID 178504064HCID 178504064, compound

Product 1

HCID 178513121HCID 178513121, compound

Reagents, catalysts & solvents 1

HCID 887MethanolSolvent

Procedure

To a solution of methyl hydrazinecarbimidothioate hydroiodide (0.100 g, 0.429 mmol) in MeOH (2 mL) was added morpholine (0.075 mL, 0.858 mmol) and refluxed overnight. Reaction was cool to RT and concentrated to get morpholine-4-carboximidhydrazide as a white solid in quantitative yield.

Workup

  1. temperaturerefluxed overnight
  2. customReaction
  3. concentrationconcentrated

Sources & evidence

ORD record
ord-6407090cb11347459dd3c8c7f1ae4f0f
Source dataset
uspto-grants-2016_01
Patent number
US09227971B2

Reaction notes

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