Ethyl Acetate → HCID 89590287, compound

Participants

Reaction Steps

Ethyl 2-[6-fluoro-1-(4-nitrobenzyl)-1H-indazol-3-yl]acetate (357 mg, 1.0 mmol) was dissolved in methanol (20 mL). 10% Pd/C(15 mg) was added, and reacted under hydrogen atmosphere for half an hour. TLC (petroleum ether:ethyl acetate=2:1) indicated that starting material disappeared. It was filtered to remove solid, rotate evaporated to dryness to remove the solvent, and the resulting solid was used for the next step directly.

Provenance & Evidence