HuagongsheHuagongshe Chemistry Print Report · For research reference only
Butyl Acrylate → Butyl (2E)-3-(4-cyanophenyl)-2-propenoate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Butyl Acrylate | HCID 8846 | — |
| Reactant | 4-Iodobenzonitrile | HCID 76467 | — |
| Product | Butyl (2E)-3-(4-cyanophenyl)-2-propenoate | HCID 11128088 | — |
Reaction Steps
4-Iodobenzonitrile (57 mg, 0.25 mmol) and n-butylacrylate (54 μL, 0.375 mmol) were coupled using the procedure described above, except the reaction was performed at 50° C., to give 100% conversion to (E)-n-butyl 3-(4-cyanophenyl)acrylate by GC analysis.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09233366B2 |
| Source dataset | uspto-grants-2016_01 |
| ORD ID | ord-e23bd2f368754b6db4ce530fdbc343ab |
| Source note | uspto-grants-2016_01 |