Butyl Acrylate → HCID 9834585, compound

HRID 589529Notes

Reaction equation

I[C:2]1[CH:7]=[CH:6][C:5]([O:8][CH3:9])=[CH:4][CH:3]=1.[CH2:10]([O:14][C:15](=[O:18])[CH:16]=[CH2:17])[CH2:11][CH2:12][CH3:13]>>[CH3:9][O:8][C:5]1[CH:6]=[CH:7][C:2](/[CH:17]=[CH:16]/[C:15]([O:14][CH2:10][CH2:11][CH2:12][CH3:13])=[O:18])=[CH:3][CH:4]=1

Participants

Reactant 2

HCID 8846Butyl Acrylate

HCID 696764-Iodoanisole

Product 1

HCID 9834585HCID 9834585, compound

Procedure

4-Iodoanisole (58 mg, 0.25 mmol) and n-butylacrylate (54 μL, 0.375 mmol) were coupled using the procedure described above to give 74% conversion to (E)-n-butyl 3-(4-methoxyphenyl)acrylate by GC analysis.

Sources & evidence

ORD record: ord-368dfa0dba3b4bb3b0ef6ea963e5eda2
Source dataset: uspto-grants-2016_01
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US09233366B2

Reaction notes

Loading…