Styrene → 13041-79-7

HRID 589532Notes

Reaction equation

I[C:2]1[CH:9]=[CH:8][C:5]([C:6]#[N:7])=[CH:4][CH:3]=1.[CH2:10]=[CH:11][C:12]1[CH:17]=[CH:16][CH:15]=[CH:14][CH:13]=1>>[C:6]([C:5]1[CH:8]=[CH:9][C:2](/[CH:10]=[CH:11]/[C:12]2[CH:17]=[CH:16][CH:15]=[CH:14][CH:13]=2)=[CH:3][CH:4]=1)#[N:7]

Participants

Reactant 2

HCID 7501Styrene

HCID 764674-Iodobenzonitrile

Product 1

HCID 537577413041-79-7

Procedure

4-Iodobenzonitrile (57 mg, 0.25 mmol) and styrene (43 μL, 0.375 mmol) were coupled using the procedure described above to give 63% conversion to (E)-4-cyanostilbene by GC analysis.

Sources & evidence

ORD record: ord-cb321c0ee4fc47f395d8b7b80866edde
Source dataset: uspto-grants-2016_01
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US09233366B2

Reaction notes

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