HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrogen Peroxide → HCID 178519824, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrogen Peroxide | HCID 784 | — |
| Reactant | 4-Chloropyridine-3-carbaldehyde | HCID 14046674 | — |
| Catalyst | Hydrochloric Acid | HCID 313 | — |
| Product | HCID 178519824 | HCID 178519824 | 80% |
Reaction Steps
Following the procedure described in MARSAIS et al. (J. Het. Chem., vol. 25, p. 81-87, 1988), compound 2 is heated for 6 h in an aqueous solution of 3 N HCl containing several drops of 3% H2O2, in order to obtain 4-hydroxypyridine-3-carboxaldehyde 4 as a colorless solid (>80%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09233931B2 |
| Source dataset | uspto-grants-2016_01 |
| ORD ID | ord-47762c9a6aaa458bb953ef534ec919c4 |
| Source note | uspto-grants-2016_01 |