HuagongsheHuagongshe Chemistry Print Report · For research reference only
(3,5-Difluorophenyl)boronic acid → HCID 178527490, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | (3,5-Difluorophenyl)boronic acid | HCID 2734338 | — |
| Reactant | HCID 178527479 | HCID 178527479 | — |
| Product | HCID 178527490 | HCID 178527490 | 34.3% |
Reaction Steps
The product was prepared according to General Procedure 3, described in Example 22, starting from 5-bromo-N-[3-(1H-tetrazol-5-yl)phenyl]thiophene-2-sulfonamide (Intermediate 17) (19 mg, 0.05 mmol) and 3,5-difluorophenylboronic acid (9 mg, 0.06 mmol) giving 7.2 mg (34%) of the title compound. MS (ESI+) calcd for C17H11F2N5O2S2 419.032222, found 419.032222.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09233946B2 |
| Source dataset | uspto-grants-2016_01 |
| ORD ID | ord-dd3d2357d0084435bdf52c0f559a75d3 |
| Source note | uspto-grants-2016_01 |