HuagongsheHuagongshe Chemistry Print Report · For research reference only
Tolylboronic acid → HCID 178423806, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Tolylboronic acid | HCID 79799 | — |
| Reactant | HCID 178527479 | HCID 178527479 | — |
| Product | HCID 178423806 | HCID 178423806 | 28% |
Reaction Steps
The product was prepared according to General Procedure 3, described in Example 22, starting from 5-bromo-N-[3-(1H-tetrazol-5-yl)phenyl]thiophene-2-sulfonamide (Intermediate 17) (19 mg, 0.05 mmol) and 4-methylbenzene boronic acid (8 mg, 0.06 mmol) giving 5.5 mg (28%) of the title compound. MS (ESI+) calcd for C18H15N5O2S2 397.066716, found 397.066596.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09233946B2 |
| Source dataset | uspto-grants-2016_01 |
| ORD ID | ord-db99e3f1ac5d4724b911aca6c8abf96f |
| Source note | uspto-grants-2016_01 |