HuagongsheHuagongshe Chemistry Print Report · For research reference only
(4-Fluoro-2-methoxyphenyl)boronic acid → HCID 178492919, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | (4-Fluoro-2-methoxyphenyl)boronic acid | HCID 2782672 | — |
| Reactant | HCID 178527479 | HCID 178527479 | — |
| Product | HCID 178492919 | HCID 178492919 | 38.5% |
Reaction Steps
The product was prepared according to General Procedure 3, described in Example 22, starting from 5-bromo-N-[3-(1H-tetrazol-5-yl)phenyl]thiophene-2-sulfonamide (Intermediate 17) (19 mg, 0.05 mmol) and 4-fluoro-2-methoxyphenylboronic acid (10 mg, 0.06 mmol) giving 8.3 mg (37%) of the title compound. MS (ESI+) calcd for C18H14FN5O3S2 431.052209, found 431.052249.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09233946B2 |
| Source dataset | uspto-grants-2016_01 |
| ORD ID | ord-aabc3af849d54566990effc2a53fca15 |
| Source note | uspto-grants-2016_01 |