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5-Fluoro-3-methylbenzo[b]thiophene-2-sulphonyl chloride → HCID 178432000、化合物
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 5-Fluoro-3-methylbenzo[b]thiophene-2-sulphonyl chloride | HCID 2774586 | — |
| 反応物 | HCID 178507542 | HCID 178507542 | — |
| 生成物 | HCID 178432000 | HCID 178432000 | 36% |
反応手順
The product was prepared according to General Procedure 1, described in Example 1, starting from 5-fluoro-3-methylbenzothiophene-2-sulfonyl chloride (Intermediate 14) (26 mg, 0.10 mmol) and 5-(3-amino-phenyl)tetrazole (31 mg, 0.19 mmol). The title compound was obtained in 36% yield (13.9 mg). MS (ESI+) calcd for C16H12FN5O2S2 389.041644, found 389.042334.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US09233946B2 |
| 出典データセット | uspto-grants-2016_01 |
| ORD ID | ord-e81738f6c1474d4689b642b53cd9f48a |
| 出典メモ | uspto-grants-2016_01 |