HuagongsheHuagongshe Chemistry Print Report · For research reference only
2,4-Dichloro-5-methylbenzene-1-sulphonyl chloride → 2,4-Dichloro-5-methyl-N-[3-(1H-tetrazol-5-yl)phenyl]benzenesulfonamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2,4-Dichloro-5-methylbenzene-1-sulphonyl chloride | HCID 119914 | — |
| Reactant | HCID 178507542 | HCID 178507542 | — |
| Product | 2,4-Dichloro-5-methyl-N-[3-(1H-tetrazol-5-yl)phenyl]benzenesulfonamide | HCID 178429733 | 24.5% |
Reaction Steps
The product was prepared according to General Procedure 1, described in Example 1, starting with 2,4-dichloro-5-methylbenzene sulfonyl chloride (14.3 mg, 0.055 mmol) and 5-(3-aminophenyl)tetrazole (8 mg, 0.05 mmol) yielding 4.7 mg (24%) of the title compound. MS (ESI+) calcd for C14H11Cl2N5O2S 383.001051, found 383.000871.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09233946B2 |
| Source dataset | uspto-grants-2016_01 |
| ORD ID | ord-13b2b43df69d4b1eacfd6f2aa3df9427 |
| Source note | uspto-grants-2016_01 |