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HRID589726

反应详情

EQUATION

反应方程式

HRID 589726 的结构方程式

REACTANTS

反应物

2
结构：O=S(=O)(Cl)c1ccc(Br)cc1C(F)(F)F
HCID2778608

4-Bromo-2-(trifluoromethyl)benzenesulfonyl chloride

C7H3BrClF3O2S

结构：Nc1cccc(-c2nnn[nH]2)c1
HCID178507542

未命名化合物

PRODUCTS

生成物

1
结构：O=S(=O)(Nc1cccc(-c2nnn[nH]2)c1)c1ccc(Br)cc1C(F)(F)F
HCID178527477

未命名化合物

收率 25%

PROCEDURE

实验过程

The product was synthesized according to General Procedure 1, described in Example 1, starting with 4-bromo-2-(trifluoromethyl)benzene sulfonyl chloride (17.8 mg, 0.055 mmol) and 5-(3-amino-phenyl)tetrazole (8 mg, 0.05 mmol) yielding 5.6 mg (25%) of the title compound. MS (ESI+) calcd for C14H9BrF3N5O2S 446.961242, found 446.961472.

WORKUP

后处理

  1. customThe product was synthesized