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HRID589727

反应详情

EQUATION

反应方程式

HRID 589727 的结构方程式

REACTANTS

反应物

2
结构：O=S(=O)(Cl)c1ccc(Br)cc1F
HCID2736310

4-Bromo-2-fluorobenzenesulfonyl chloride

C6H3BrClFO2S

结构：Nc1cccc(-c2nnn[nH]2)c1
HCID178507542

未命名化合物

PRODUCTS

生成物

1
结构：O=S(=O)(Nc1cccc(-c2nnn[nH]2)c1)c1ccc(Br)cc1F
HCID178527478

未命名化合物

收率 52.2%

PROCEDURE

实验过程

The product was synthesized according to General Procedure 1, described in Example 1, starting with 4-bromo-2-fluorobenzene sulfonyl chloride (17.8 mg, 0.055 mmol) and 5-(3-aminophenyl)tetrazole (8 mg, 0.05 mmol) affording 10.4 mg (52%) of the title compound. MS (ESI+) calcd for C13H9BrFN5O2S 396.964436, found 396.963956.

WORKUP

后处理

  1. customThe product was synthesized