HuagongsheHuagongshe Chemistry Print Report · For research reference only
2,4,5-Trichlorobenzenesulfonyl chloride → HCID 178527509, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2,4,5-Trichlorobenzenesulfonyl chloride | HCID 27575 | — |
| Reactant | HCID 178507542 | HCID 178507542 | — |
| Product | HCID 178527509 | HCID 178527509 | 57% |
Reaction Steps
The product was prepared according to General Procedure 6, described in Example 65, with 2,4,5-trichlorobenzenesulfonyl chloride (15.4 mg, 0.055 mmol) and 5-(3-aminophenyl)tetrazole (8.0 mg, 0.050 mmol). The title compound was obtained in 57% yield (11.4 mg). MS (ESI+) calcd mass for C13H8Cl3N5O2S 402.946428, found 402.946388.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09233946B2 |
| Source dataset | uspto-grants-2016_01 |
| ORD ID | ord-3ce9140ace074024abd18ac5a8aed482 |
| Source note | uspto-grants-2016_01 |