HuagongsheHuagongshe Chemistry Print Report · For research reference only
2,4-Difluorobenzenesulfonyl Chloride → HCID 178527507, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2,4-Difluorobenzenesulfonyl Chloride | HCID 2734273 | — |
| Reactant | HCID 178507542 | HCID 178507542 | — |
| Product | HCID 178527507 | HCID 178527507 | 56% |
Reaction Steps
The product was prepared according to General Procedure 6, described in Example 65, with 2,4-difluorobenzenesulfonyl chloride (11.7 mg, 0.055 mmol) and 5-(3-amino-phenyl)tetrazole (8.0 mg, 0.050 mmol). The title compound was obtained in 56% yield (9.5 mg). MS (ESI+) calcd mass for C13H9F2N5O2S 337.044502, found 337.044202.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09233946B2 |
| Source dataset | uspto-grants-2016_01 |
| ORD ID | ord-0e9233015ecc4f41b5ad75d4f1bd57cc |
| Source note | uspto-grants-2016_01 |