3-Aminobenzoic Acid → 3-{[(3-Methyl-1-benzothiophen-2-yl)sulfonyl]amino}benzoic acid

Beteiligte Stoffe

Reaktionsschritte

The product was prepared according to General Procedure 1, described in Example 1, with 3-methylbenzothiophene-2-sulfonyl chloride (Intermediate 11) (25 mg, 0.10 mmol) and 3-aminobenzoic acid (28 mg, 0.20 mmol) using a modified reaction time (4 hours) and a modified reaction temperature (60° C.). The title compound was obtained in 26% yield (8.9 mg). MS (ESI+) calcd mass for C16H13NO4S2 347.028599, found 347.028659.

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