HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Chloro-4-fluorobenzene-1-sulfonyl chloride → HCID 178527506, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Chloro-4-fluorobenzene-1-sulfonyl chloride | HCID 522846 | — |
| Reactant | HCID 178507542 | HCID 178507542 | — |
| Product | HCID 178527506 | HCID 178527506 | 62% |
Reaction Steps
The product was prepared according to General Procedure 6, described in Example 65, with 2-chloro-4-fluorobenzenesulfonyl chloride (12.6 mg, 0.055 mmol) and 5-(3-aminophenyl)tetrazole (8.0 mg, 0.050 mmol). The title compound was obtained in 62% yield (10.9 mg). MS (ESI+) calcd mass for C13H9ClFN5O2S 353.014951, found 353.015041.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09233946B2 |
| Source dataset | uspto-grants-2016_01 |
| ORD ID | ord-d139f8fff2af4056a5f4860f2a9ab6fa |
| Source note | uspto-grants-2016_01 |