HuagongsheHuagongshe Chemistry Print Report · For research reference only
(3-Chlorophenyl)boronic acid → HCID 178527484, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | (3-Chlorophenyl)boronic acid | HCID 2734323 | — |
| Reactant | HCID 178527479 | HCID 178527479 | — |
| Product | HCID 178527484 | HCID 178527484 | 26% |
Reaction Steps
The product was prepared according to General Procedure 3, described in Example 22, using 5-bromo-N-[3-(1H-tetrazol-5-yl)phenyl]thiophene-2-sulfonamide (Intermediate 17) (19 mg, 0.055 mmol) and 3-chlorophenylboronic acid (9 mg, 0.06 mmol). The title compound was obtained in 26% yield (5.4 mg). MS (ESI+) calcd mass for C17H12ClN5O2S2 417.012094, found 417.012844.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09233946B2 |
| Source dataset | uspto-grants-2016_01 |
| ORD ID | ord-dac168a59c1e41d88015930336f4d4ff |
| Source note | uspto-grants-2016_01 |