HuagongsheHuagongshe Chemistry Print Report · For research reference only
5-Bromo-2-chlorobenzoic acid → HCID 79795128, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 5-Bromo-2-chlorobenzoic acid | HCID 33127 | — |
| Reactant | 5-Methylpyridine-2,3-diamine | HCID 10701825 | — |
| Product | HCID 79795128 | HCID 79795128 | — |
Reaction Steps
Intermediate I-4 was synthesized in a similar fashion as described in the synthesis of I-2a using 5-methylpyridine-2,3-diamine and 5-bromo-2-chlorobenzoic acid. 1H NMR (400 MHz, DMSO) δ 8.18 (d, J=2.4 Hz, 1H), 8.07 (s, 1H), 7.68 (s, 1H), 7.60 (dd, J=2.2, 8.4 Hz, 1H), 7.51 (d, J=8.5 Hz, 1H), 2.39 (s, 3H). MS M/Z=322/324 (M+1).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09233961B2 |
| Source dataset | uspto-grants-2016_01 |
| ORD ID | ord-4e169ac0bb41456c8376460194d1f500 |
| Source note | uspto-grants-2016_01 |