反应详情

Sulfuryl chloride (104 mmol) was dissolved in dry CH3CN (25 mL), added cyclobutylamine hydrochloride (31 mmol) and stirred at reflux for 16 h. The obtained reaction mixture was cooled to rt and concentrated in vacuo. The obtained residue was trituated with Et2O (2×25 mL). The combined Et2O-phases were concentrated in vacuo affording the title compound as oil.

1. temperatureat reflux for 16 h
2. customThe obtained reaction mixture
3. concentrationconcentrated in vacuo
4. concentrationThe combined Et2O-phases were concentrated in vacuo