Ammonia → HCID 178463316, compound

Participants

Reaction Steps

To a solution of 0.002 mol (429 mg) of N-ethyl-N-isopropyl-4-aminoaniline hydrochloride and 0.001 mol (124 mg) of orcinol in 2 ml of water and 6 ml of ethanol brought to a pH of 9.5 with a solution of 20% aqueous ammonia, 0.002 mol (456 mg) of ammonium persulfate dissolved in 1 ml of water is added dropwise. The temperature is held below 30° C. during the addition. At the end of the addition, the precipitate formed is filtered and washed with water.

Provenance & Evidence