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Methyl 3-amino-2-methylpropanoate hydrochloride → Methyl 1-(aminomethyl)cyclopropane-1-carboxylate--hydrogen chloride (1/1)
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Methyl 3-amino-2-methylpropanoate hydrochloride | HCID 13063725 | — |
| 反応物 | 1-(Aminomethyl)cyclopropanecarboxylic acid | HCID 15033901 | — |
| 生成物 | Methyl 1-(aminomethyl)cyclopropane-1-carboxylate--hydrogen chloride (1/1) | HCID 21464884 | — |
反応手順
The title compound was prepared in analogy to Compound W in Example 20 by using 1-(aminomethyl)cyclopropanecarboxylic acid (CAS number: 139132-50-6, J&K; for its synthesis, please refer to: Mertin A., et al. Synlett, 1991, 2, 87-9) instead of DL-3-aminoisobutyric acid.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US09233978B2 |
| 出典データセット | uspto-grants-2016_01 |
| ORD ID | ord-371ed32666a142eca0c49046322d6718 |
| 出典メモ | uspto-grants-2016_01 |