Dimethyl Sulfoxide → HCID 88244284, compound

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Reaction Steps

To a separate flask under an inert atmosphere was added 9-bromoethylanthracene, 10 mL anhydrous THF, and 5 mL anhydrous dimethylsulfoxide. The resulting mixture was added to the solution prepared above. The resulting reaction mixture was then stirred for 15 hrs at room temperature. The mixture was then slowly quenched using saturated NaHCO3. The products were extracted with dichloromethane and dried over sodium sulfate. The solvents were evaporated under reduced pressure and purified using flash column chromatography.

Provenance & Evidence