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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 590665Generated: October 30, 2026

HCID 67386995, compound → HCID 15719911, compound

https://huagongshe.com/reaction/590665

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 67386995HCID 67386995—
CatalystPalladiumHCID 23938—
SolventEthanolHCID 702—
ProductHCID 15719911HCID 1571991197%

Reaction Steps

A mixture of (S)-1-tert-butyl 2-methyl 4-ethylidenepyrrolidine-1,2-dicarboxylate (50 g, 196 mmol), Pd/C (5 g) in EtOH (500 mL) was hydrogenated at room temperature overnight. The mixture was filtered and concentrated to afford (2S)-1-tert-butyl 2-methyl 4-ethylpyrrolidine-1,2-dicarboxylate (9.8 g, 97%) as colorless oil.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS09233974B2
Source datasetuspto-grants-2016_01
ORD IDord-20f9db38991b45abb873eb68c9d892ff
Source noteuspto-grants-2016_01