Benzoyl chloride, 3-nitro- → N-(2-iodo-4-(perfluoropropan-2-yl)-6-(trifluoromethyl)phenyl)-3-nitrobenzamide

HRID 590932Notes

Reaction equation

HRID 590932 reaction equation
[I:1][C:2]1[CH:8]=[C:7]([C:9]([F:18])([C:14]([F:17])([F:16])[F:15])[C:10]([F:13])([F:12])[F:11])[CH:6]=[C:5]([C:19]([F:22])([F:21])[F:20])[C:3]=1[NH2:4].[N+:23]([C:26]1[CH:27]=[C:28]([CH:32]=[CH:33][CH:34]=1)[C:29](Cl)=[O:30])([O-:25])=[O:24]>>[I:1][C:2]1[CH:8]=[C:7]([C:9]([F:18])([C:10]([F:11])([F:12])[F:13])[C:14]([F:15])([F:16])[F:17])[CH:6]=[C:5]([C:19]([F:20])([F:21])[F:22])[C:3]=1[NH:4][C:29](=[O:30])[C:28]1[CH:32]=[CH:33][CH:34]=[C:26]([N+:23]([O-:25])=[O:24])[CH:27]=1

Participants

3

Reactant 2

HCID 8495Benzoyl chloride, 3-nitro-HCID 582975324-(1,1,1,2,3,3,3-Heptafluoropropan-2-yl)-2-iodo-6-(trifluoromethyl)aniline

Product 1

HCID 86654235N-(2-iodo-4-(perfluoropropan-2-yl)-6-(trifluoromethyl)phenyl)-3-nitrobenzamide

Procedure

According to the method of 4-3 of Example 4, a target compound was prepared from 2-iodo-4-(perfluoropropan-2-yl)-6-(trifluoromethyl)aniline and 3-nitrobenzoyl chloride.

Sources & evidence

ORD record
ord-c8cf64cdc5fd43a199d276813c4c476c
Source dataset
uspto-grants-2016_01
Patent number
US09237745B2

Reaction notes

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