2-Chloro-3-nitrobenzoyl chloride → 2-chloro-N-(2-iodo-4-(heptafluoropropan-2-yl)-6-(trifluoromethyl)phenyl)-3-nitrobenzamide

HRID 590944Notes

Reaction equation

HRID 590944 reaction equation
[I:1][C:2]1[CH:8]=[C:7]([C:9]([F:18])([C:14]([F:17])([F:16])[F:15])[C:10]([F:13])([F:12])[F:11])[CH:6]=[C:5]([C:19]([F:22])([F:21])[F:20])[C:3]=1[NH2:4].[Cl:23][C:24]1[C:32]([N+:33]([O-:35])=[O:34])=[CH:31][CH:30]=[CH:29][C:25]=1[C:26](Cl)=[O:27]>>[Cl:23][C:24]1[C:32]([N+:33]([O-:35])=[O:34])=[CH:31][CH:30]=[CH:29][C:25]=1[C:26]([NH:4][C:3]1[C:5]([C:19]([F:20])([F:21])[F:22])=[CH:6][C:7]([C:9]([F:18])([C:10]([F:11])([F:12])[F:13])[C:14]([F:15])([F:16])[F:17])=[CH:8][C:2]=1[I:1])=[O:27]

Participants

3

Reactant 2

HCID 126274132-Chloro-3-nitrobenzoyl chlorideHCID 582975324-(1,1,1,2,3,3,3-Heptafluoropropan-2-yl)-2-iodo-6-(trifluoromethyl)aniline

Product 1

HCID 866566962-chloro-N-(2-iodo-4-(heptafluoropropan-2-yl)-6-(trifluoromethyl)phenyl)-3-nitrobenzamide

Procedure

According to the method of 3-2 of Example 3, a target compound was prepared from 2-iodo-4-(heptafluoropropan-2-yl)-6-(trifluoromethyl)aniline and 2-chloro-3-nitrobenzoyl chloride.

Sources & evidence

ORD record
ord-ad591b61d5c442998aed9b21636ebbca
Source dataset
uspto-grants-2016_01
Patent number
US09237745B2

Reaction notes

Loading…