Sodium ethoxide → HCID 51347396, compound

Participants

Reaction Conditions

Reaction Steps

Intermediate 10 (0.15 g, 0.349 mmol) was added to sodium ethoxide (ALDRICH, 0.071 g, 1.048 mmol) in ethanol (3 mL). The mixture was heated under microwave irradiation at 120° C. for 30 minutes. Solvent was removed under vacuum and the crude mixture was purified by flash chromatography (Si, eluting with DCM: MeOH mixtures from 100:0 to 90:10%). The title compound was obtained as a white solid.

Provenance & Evidence