HuagongsheHuagongshe Chemistry Print Report · For research reference only
Triphenylphosphine → ((2,6-Dimethylpyridin-3-yl)methyl)(triphenyl)phosphonium chloride
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Triphenylphosphine | HCID 11776 | — |
| Reactant | 3-(Chloromethyl)-2,6-dimethylpyridine | HCID 62830608 | — |
| Solvent | Acetonitrile | HCID 6342 | — |
| Product | ((2,6-Dimethylpyridin-3-yl)methyl)(triphenyl)phosphonium chloride | HCID 118656271 | 78.9% |
Reaction Steps
A mixture of triphenylphosphine (885 mg), 3-(chloromethyl)-2,6-dimethylpyridine (500 mg) and CH3CN (20 mL) was refluxed for 24 h. The mixture was concentrated in vacuo. The residual solid was washed with IPE to give the title compound (1060 mg).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09238639B2 |
| Source dataset | uspto-grants-2016_01 |
| ORD ID | ord-33f37836e8e848dba1d4b8598cc458b3 |
| Source note | uspto-grants-2016_01 |