HCID 71721661, compound → HCID 118667045, compound

Participants

Reaction Steps

A mixture of ethyl(6-((Z)-2-(2,6-dimethylpyridin-3-yl)vinyl)-1-benzothiophen-3-yl)acetate (110 mg), 10% Pd—C (50% wet, 50 mg) and THF (5 mL) was hydrogenated under atmospheric pressure for 30 min. The catalyst was removed by filtration. The filtrate was concentrated in vacuo. The residue was purified by silica gel column chromatography (EtOAc/hexane) to give the title compound (90 mg).

Provenance & Evidence