Ethyl isocyanate → HCID 89767872, compound

Participants

Reaction Conditions

Reaction Steps

To a mixture of 6-((2,4-dichlorobenzyl)oxy)-2,3-dihydro-1-benzofuran-3-amine (146 mg) and THF (dry) (4.0 mL) was added ethyl isocyanate (0.048 mL) at 0° C. The mixture was stirred at 0° C. for 1 h. The mixture was poured into saturated aqueous NH4Cl at 0° C. and extracted with EtOAc. The organic layer was m washed with brine, dried over MgSO4, and concentrated in vacuo. The solid was washed with EtOH to give the title compound (74.0 mg).

Provenance & Evidence