Trimethyl orthoformate → HCID 66690797, compound

Participants

Role	Name	HCID	Charge
Reactant	Trimethyl orthoformate	HCID 9005	—
Reactant	HCID 66690636	HCID 66690636	—
Product	HCID 66690797	HCID 66690797	—

Reaction Conditions

Temperature	85 °C

Reaction Steps

Trimethyl orthoformate (19 mL, 172 mmol) was added neat to tert-butyl 5-chloro-6-hydrazinonicotinate (1.9 g, 7.8 mmol). The mixture was heated to 85° C. After 4 h, the mixture was cooled to ambient temperature and concentrated to dryness: LC-MS [M+1]=254.1.

Provenance & Evidence

DOI	10.6084/m9.figshare.5104873.v1
Patent number	US09238647B2
Source dataset	uspto-grants-2016_01
ORD ID	ord-860a9222978149548ad989cd76d51d3f
Source note	uspto-grants-2016_01