HuagongsheHuagongshe Chemistry Print Report · For research reference only
Pyrrolidine → (E)-1-(4-bromo-2-nitrostyryl)pyrrolidine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Pyrrolidine | HCID 31268 | — |
| Reactant | Dimethylformamide dimethyl acetal | HCID 78373 | — |
| Reactant | 4-Bromo-2-nitrotoluene | HCID 123546 | — |
| Product | (E)-1-(4-bromo-2-nitrostyryl)pyrrolidine | HCID 10913500 | — |
Reaction Steps
A solution of 4-bromo-2-nitrotoluene (100 g, 463 mmol), pyrrolidine (46.2 mL, 565 mmol), and N,N-dimethylformamide dimethylacetal (75.6 mL, 565 mmol) was refluxed for 4 hours at
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09242964B2 |
| Source dataset | uspto-grants-2016_01 |
| ORD ID | ord-fedbb09e7477404eb57e50e8f2acf982 |
| Source note | uspto-grants-2016_01 |