HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
1-Bromo-2-methylpropane → N-(3,5-dimethylpyridin-2-yl)-4-fluoro-N-isobutylbenzenesulfonamide
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | 1-Bromo-2-methylpropane | HCID 6555 | — |
| Edukt | N-(3,5-dimethylpyridin-2-yl)-4-fluorobenzenesulfonamide | HCID 89876077 | — |
| Produkt | N-(3,5-dimethylpyridin-2-yl)-4-fluoro-N-isobutylbenzenesulfonamide | HCID 89876058 | 53,2% |
Reaktionsschritte
The title compound (53.7 mg) was prepared from N-(3,5-dimethylpyridin-2-yl)-4-fluorobenzenesulfonamide (84 mg, 0.300 mmol) and 1-bromo-2-methylpropane (0.065 mL, 0.599 mmol), following procedure described for Example 22. LCMS (2 min, formic) Rt 0.96 min, m/z (ES+) 337 (M+H).
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US09242972B2 |
| Quelldatensatz | uspto-grants-2016_01 |
| ORD ID | ord-fa07053d27a74eb8a24d1e17dacfc942 |
| Quellennotiz | uspto-grants-2016_01 |