Methanol → HCID 107908220, compound

Participants

Reaction Steps

To a solution of 5-bromothiazol-2-amine bromate (1 g) in methylene chloride (12 mL) was added a solution of pyridine (0.68 mL) and 5-bromopentanoyl chloride (0.54 mL) in methylene chloride (0.7 mL). The reaction mixture was stirred at room temperature for 2 hours. The reaction mixture was added with methanol (0.7 mL) and concentrated under reduced pressure. The obtained residue was added with 1 N hydrochloric acid (13 mL). The obtained solid was washed with tert-butyl methyl ether and dried to give the titled compound (1.06 g) having the following physical data.

Provenance & Evidence