HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-(1H-1,2,4-Triazol-1-yl)benzaldehyde → HCID 69080170, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-(1H-1,2,4-Triazol-1-yl)benzaldehyde | HCID 18525741 | — |
| Reactant | Methyl 5-amino-5-(2,6-dimethoxyphenyl)pentanoate | HCID 69082713 | — |
| Product | HCID 69080170 | HCID 69080170 | — |
Reaction Steps
Prepared according to the described general procedure 1 (GP1) by reaction of methyl 5-amino-5-(2,6-dimethoxyphenyl)pentanoate with commercially available 3-(1H-1,2,4-triazol-1-yl)benzaldehyde. Subsequent purification by preparative HPLC afforded the target compound. LC-MS (conditions A): tR=0.70 min.; [M+H]+: 393.15 g/mol.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09242970B2 |
| Source dataset | uspto-grants-2016_01 |
| ORD ID | ord-b307d42aa7124d1199d5fbccd3348c44 |
| Source note | uspto-grants-2016_01 |