HuagongsheHuagongshe Chemistry Print Report · For research reference only
1,3-Benzothiazole-2-carbaldehyde → HCID 86695636, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1,3-Benzothiazole-2-carbaldehyde | HCID 241608 | — |
| Reactant | Methyl 5-amino-5-(2,6-dimethoxyphenyl)pentanoate | HCID 69082713 | — |
| Product | HCID 86695636 | HCID 86695636 | — |
Reaction Steps
Prepared according to the described general procedure 1 (GP1) by reaction of methyl 5-amino-5-(2,6-dimethoxyphenyl)pentanoate with commercially available benzo[d]thiazole-2-carbaldehyde. Subsequent purification by preparative HPLC afforded the target compound. LC-MS (conditions A): tR=0.82 min.; [M+H]+: 383.14 g/mol.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09242970B2 |
| Source dataset | uspto-grants-2016_01 |
| ORD ID | ord-d753c3c4490e4e91aa8aaddbe528ce8b |
| Source note | uspto-grants-2016_01 |