HuagongsheHuagongshe Chemistry Print Report · For research reference only
[2,2'-Bipyridine]-4-carbaldehyde → HCID 69082428, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | [2,2'-Bipyridine]-4-carbaldehyde | HCID 10171298 | — |
| Reactant | Methyl 5-amino-5-(2,6-dimethoxyphenyl)pentanoate | HCID 69082713 | — |
| Product | HCID 69082428 | HCID 69082428 | — |
Reaction Steps
Prepared according to the described general procedure 1 (GP1) by reaction of methyl 5-amino-5-(2,6-dimethoxyphenyl)pentanoate with [2,2′-bipyridine]-4-carbaldehyde. Subsequent purification by preparative HPLC afforded the target compound. LC-MS (conditions A): tR=0.59 min.; [M+H]+: 403.97 g/mol.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09242970B2 |
| Source dataset | uspto-grants-2016_01 |
| ORD ID | ord-ee44527a513a451b850a9e74f7358db9 |
| Source note | uspto-grants-2016_01 |