HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Methyl-1,3-thiazole-4-carbaldehyde → HCID 69084084, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Methyl-1,3-thiazole-4-carbaldehyde | HCID 2763191 | — |
| Reactant | Methyl 5-amino-5-(2,6-dimethoxyphenyl)pentanoate | HCID 69082713 | — |
| Product | HCID 69084084 | HCID 69084084 | — |
Reaction Steps
Prepared according to the described general procedure 1 (GP1) by reaction of methyl 5-amino-5-(2,6-dimethoxyphenyl)pentanoate with commercially available 2-methylthiazole-4-carbaldehyde. Subsequent purification by preparative HPLC afforded the target compound. LC-MS (conditions A): tR=0.65 min.; [M+H]+: 346.85 g/mol.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09242970B2 |
| Source dataset | uspto-grants-2016_01 |
| ORD ID | ord-0899929400bb4f52a679c72ae4fef69e |
| Source note | uspto-grants-2016_01 |