huagongshe.com
HRID594509

反应详情

EQUATION

反应方程式

HRID 594509 的结构方程式

REACTANTS

反应物

2
结构：Cc1nc(-c2cccc(C=O)c2)cs1
HCID7127782

3-(2-methyl-1,3-thiazol-4-yl)benzaldehyde

C11H9NOS

结构：COC(=O)CCCCC(N)c1c(OC)cccc1OC
HCID69082587

未命名化合物

PRODUCTS

生成物

1
结构：COc1cccc(OC)c1C1CCCCC(=O)N1Cc1cccc(-c2csc(C)n2)c1
HCID69082689

未命名化合物

PROCEDURE

实验过程

Prepared according to the described general procedure 1 (GP1) by reaction of methyl 6-amino-6-(2,6-dimethoxyphenyl)hexanoate with commercially available 3-(2-methylthiazol-4-yl)benzaldehyde. Subsequent purification by preparative HPLC afforded the target compound. LC-MS (conditions I): tR=1.37 min.; [M+H]+: 437.10 g/mol.

WORKUP

后处理

  1. customPrepared
  2. customSubsequent purification by preparative HPLC
  3. customafforded the target compound