HuagongsheHuagongshe Chemistry Print Report · For research reference only
6-Phenylpyridine-2-carbaldehyde → HCID 69082588, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 6-Phenylpyridine-2-carbaldehyde | HCID 13522416 | — |
| Reactant | Ethyl 4-amino-4-(2,6-dimethoxyphenyl)-2-methylbutanoate | HCID 69085588 | — |
| Product | HCID 69082588 | HCID 69082588 | — |
Reaction Steps
Prepared according to the described general procedure 2 (GP2) by reaction of ethyl 4-amino-4-(2,6-dimethoxyphenyl)-2-methylbutanoate with 6-phenylpicolinaldehyde. Subsequent purification by preparative HPLC afforded the target compound. LC-MS (conditions A): tR=0.82 min.; [M+H]+: 403.00 g/mol.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09242970B2 |
| Source dataset | uspto-grants-2016_01 |
| ORD ID | ord-b887864c4b5d4b7abcab6b85ccbe7cb1 |
| Source note | uspto-grants-2016_01 |