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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 594560Generated: October 26, 2026

3-(Pyrimidin-2-yl)benzaldehyde → HCID 69082703, compound

https://huagongshe.com/reaction/594560

Reaction equation

Participants

RoleNameHCIDCharge
Reactant3-(Pyrimidin-2-yl)benzaldehydeHCID 22630818—
ReactantEthyl 4-amino-4-(2,6-dimethoxyphenyl)-2-methylbutanoateHCID 69085588—
ProductHCID 69082703HCID 69082703—

Reaction Steps

Prepared according to the described general procedure 2 (GP2) by reaction of ethyl 4-amino-4-(2,6-dimethoxyphenyl)-2-methylbutanoate with commercially available 3-(pyrimidin-2-yl)benzaldehyde. Subsequent purification by preparative HPLC afforded the target compound. LC-MS (conditions A): tR=0.79 min.; [M+H]+: 403.86 g/mol.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS09242970B2
Source datasetuspto-grants-2016_01
ORD IDord-0aa9851b671741ff8dc5dbe9f787ae92
Source noteuspto-grants-2016_01