HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-(Bromomethyl)-1-benzofuran → HCID 69083788, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-(Bromomethyl)-1-benzofuran | HCID 12326316 | — |
| Reactant | 6-(2,6-Dimethoxyphenyl)piperidin-2-one | HCID 69082526 | — |
| Product | HCID 69083788 | HCID 69083788 | — |
Reaction Steps
Prepared according to the described general procedure 4 (GP4) by reaction of 6-(2,6-dimethoxyphenyl)piperidin-2-one with 2-(bromomethyl)benzofuran. Subsequent purification by preparative HPLC afforded the target compound. LC-MS (conditions F): tR=0.83 min.; [M+H]+: 366.15 g/mol.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09242970B2 |
| Source dataset | uspto-grants-2016_01 |
| ORD ID | ord-47a6339cbf554cba9b97f63702cd2570 |
| Source note | uspto-grants-2016_01 |