2,6-Dimethoxybenzaldehyde → HCID 69085295, compound

HRID 594640Notes

Reaction equation

HRID 594640 reaction equation
[C:1]1([C:9]2[CH:14]=[CH:13][CH:12]=[CH:11][CH:10]=2)[CH:6]=[CH:5][C:4]([CH2:7][NH2:8])=[CH:3][CH:2]=1.[CH3:15][O:16][C:17]1[CH:24]=[CH:23][CH:22]=[C:21]([O:25][CH3:26])[C:18]=1[CH:19]=O>>[C:1]1([C:9]2[CH:10]=[CH:11][CH:12]=[CH:13][CH:14]=2)[CH:2]=[CH:3][C:4]([CH2:7][N:8]2[CH:19]([C:18]3[C:17]([O:16][CH3:15])=[CH:24][CH:23]=[CH:22][C:21]=3[O:25][CH3:26])[CH2:22][CH2:21][CH2:18][C:17]2=[O:16])=[CH:5][CH:6]=1

Participants

3

Reactant 2

HCID 964042,6-DimethoxybenzaldehydeHCID 3449894-Phenylbenzylamine

Product 1

HCID 69085295HCID 69085295, compound

Procedure

Prepared according to the described general procedure 6 (GP6) with commercially available [1,1′-biphenyl]-4-ylmethanamine and commercially available 2,6-dimethoxybenzaldehyde. Subsequent purification by preparative HPLC afforded the target compound. LC-MS (conditions E): tR=0.84 min.; [M+H]+: 401.85 g/mol.

Workup

  1. customPrepared
  2. customSubsequent purification by preparative HPLC
  3. customafforded the target compound

Sources & evidence

ORD record
ord-dbe175c52bb9445e85d6fb8cfec89f03
Source dataset
uspto-grants-2016_01
Patent number
US09242970B2

Reaction notes

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