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HRID594675

反应详情

EQUATION

反应方程式

HRID 594675 的结构方程式

REACTANTS

反应物

2
结构：Cc1nc(-c2cccc(C=O)c2)cs1
HCID7127782

3-(2-methyl-1,3-thiazol-4-yl)benzaldehyde

C11H9NOS

结构：CCOC(=O)C(C)CC(N)c1ccccc1-c1ccccc1
HCID69082640

未命名化合物

PRODUCTS

生成物

1
结构：Cc1nc(-c2cccc(CN3C(=O)C(C)CC3c3ccccc3-c3ccccc3)c2)cs1
HCID69083752

未命名化合物

PROCEDURE

实验过程

Prepared according to the described general procedure 2 (GP2) by reaction of ethyl 4-([1,1′-biphenyl]-2-yl)-4-amino-2-methylbutanoate with commercially available 3-(2-methylthiazol-4-yl)benzaldehyde. Subsequent purification by preparative HPLC afforded the target compound. LC-MS (conditions A): tR=0.97 min.; [M+H]+: 439.03 g/mol.

WORKUP

后处理

  1. customPrepared
  2. customSubsequent purification by preparative HPLC
  3. customafforded the target compound