HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dibenzo(b,d)furan-2-carboxaldehyde → HCID 86695659, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dibenzo(b,d)furan-2-carboxaldehyde | HCID 220843 | — |
| Reactant | Ethyl 4-amino-4-(2-ethoxy-6-fluorophenyl)-2-methylbutanoate | HCID 69083532 | — |
| Product | HCID 86695659 | HCID 86695659 | — |
Reaction Steps
Prepared according to the described general procedure 2 (GP2) by reaction of ethyl 4-amino-4-(2-ethoxy-6-fluorophenyl)-2-methylbutanoate with commercially available dibenzo[b,d]furan-2-carbaldehyde. Subsequent purification by preparative HPLC afforded the target compound. LC-MS (conditions A): tR=1.00 min.; [M+H]+: 417.81 g/mol.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09242970B2 |
| Source dataset | uspto-grants-2016_01 |
| ORD ID | ord-15f9a44813844789bf0ec995ec9f8f40 |
| Source note | uspto-grants-2016_01 |