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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 594721Generated: October 29, 2026

5-Fluoro-1-methyl-1H-indole-2-carbaldehyde → HCID 69082472, compound

https://huagongshe.com/reaction/594721

Reaction equation

Participants

RoleNameHCIDCharge
Reactant5-Fluoro-1-methyl-1H-indole-2-carbaldehydeHCID 23004696—
ReactantEthyl 4-amino-4-(2,6-dimethoxyphenyl)-2-methylbutanoateHCID 69085588—
ProductHCID 69082472HCID 69082472—

Reaction Steps

Prepared according to the described general procedure 2 (GP2) by reaction of ethyl 4-amino-4-(2,6-dimethoxyphenyl)-2-methylbutanoate with commercially available 5-fluoro-1-methyl-1H-indole-2-carbaldehyde. Subsequent purification by preparative HPLC afforded the target compound. LC-MS (conditions A): tR=0.90 min.; [M+H]+: 397.08 g/mol.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS09242970B2
Source datasetuspto-grants-2016_01
ORD IDord-0c5e6adb021440e98f5aa1baae624fb6
Source noteuspto-grants-2016_01