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HRID594724

反应详情

EQUATION

反应方程式

HRID 594724 的结构方程式

REACTANTS

反应物

2
结构：Cc1nc2cc(C=O)ccc2s1
HCID2308820

2-Methylbenzo[d]thiazole-5-carbaldehyde

C9H7NOS

结构：CCOC(=O)C(C)CC(N)c1c(OC)cccc1OC
HCID69085588

未命名化合物

PRODUCTS

生成物

1
结构：COc1cccc(OC)c1C1CC(C)C(=O)N1Cc1ccc2sc(C)nc2c1
HCID76324989

未命名化合物

PROCEDURE

实验过程

Prepared according to the described general procedure 2 (GP2) by reaction of ethyl 4-amino-4-(2,6-dimethoxyphenyl)-2-methylbutanoate with 2-methylbenzo[d]thiazole-5-carbaldehyde. Subsequent purification by preparative HPLC afforded the target compound. LC-MS (conditions A): tR=0.79 min.; [M+H]+: 396.76 g/mol.

WORKUP

后处理

  1. customPrepared
  2. customSubsequent purification by preparative HPLC
  3. customafforded the target compound