HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzaldehyde, 3-(1,1,2,2-tetrafluoroethoxy)- → HCID 86695666, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzaldehyde, 3-(1,1,2,2-tetrafluoroethoxy)- | HCID 118803 | — |
| Reactant | Ethyl 4-amino-4-(2,6-dimethoxyphenyl)-2-methylbutanoate | HCID 69085588 | — |
| Product | HCID 86695666 | HCID 86695666 | — |
Reaction Steps
Prepared according to the described general procedure 2 (GP2) by reaction of ethyl 4-amino-4-(2,6-dimethoxyphenyl)-2-methylbutanoate with commercially available 3-(1,1,2,2-tetrafluoroethoxy)benzaldehyde. Subsequent purification by preparative HPLC afforded the target compound. LC-MS (conditions A): tR=0.90 min.; [M+H]+: 441.98 g/mol.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09242970B2 |
| Source dataset | uspto-grants-2016_01 |
| ORD ID | ord-b1663acc125b4239a99fd6d436dccae4 |
| Source note | uspto-grants-2016_01 |